4-(Octyloxy)benzoic acid → 4-Octyloxybenzoyl chloride

HRID 729105

Reaction equation

HRID 729105 reaction equation
[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][C:13]([C:14](O)=[O:15])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:21])=O>C1C=CC=CC=1>[CH2:1]([O:9][C:10]1[CH:18]=[CH:17][C:13]([C:14]([Cl:21])=[O:15])=[CH:12][CH:11]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 172314-(Octyloxy)benzoic acidHCID 24386Thionyl Chloride

Product 1

HCID 27602504-Octyloxybenzoyl chloride

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

4-n-Octyloxybenzoic acid in the amount of 2.0 g was reacted with 1 g of thionyl chloride in 10 ml of benzene at a temperature of 100°-110° C. for 6 hours to obtain 4-n-octyloxybenzoic chloride in the amount of 2.2 g.

Sources & evidence

ORD record
ord-866c43c2eb044e5dac6491b551d06f4c
Source dataset
uspto-grants-1991_09
Patent number
US05051527

Linked notes

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