HCID 12256609, compound → HCID 69053135, compound

Reaction equation

[Cl:1][CH2:2][CH2:3][CH2:4][C:5]1[CH:10]=[CH:9][C:8]([S:11][CH3:12])=[CH:7][CH:6]=1.ClCCC1C=CC(S(C)=[O:23])=CC=1>>[Cl:1][CH2:2][CH2:3][CH2:4][C:5]1[CH:6]=[CH:7][C:8]([S:11]([CH3:12])=[O:23])=[CH:9][CH:10]=1

Participants

Reactant 2

HCID 12256609HCID 12256609, compound

HCID 69054714HCID 69054714, compound

Product 1

HCID 69053135HCID 69053135, compound

Procedure

12b was prepared from 11b (2.0 g; 10.0 mmol) using the method described in the synthesis of 12a. M.p.: 46° C.

Sources & evidence

ORD record: ord-9d0e65bbfeef43e7ba502a14b564c336
Source dataset: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07582660B2

Reaction notes

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