HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Biphenyl-3-ylmethylamine hydrobromide → N-(1,1'-biphenyl-3-ylmethyl)-N-[3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Biphenyl-3-ylmethylamine hydrobromide | HCID 67188044 | — |
| Reactant | 3-(3-Undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde | HCID 86598538 | — |
| Product | N-(1,1'-biphenyl-3-ylmethyl)-N-[3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzyl]amine | HCID 67188008 | — |
Reaction Steps
The same procedure as employed in the preparation of Example 357 (step a) but using 3-(3-undecyl-1,2,4-oxadiazol-5-yl)benzaldehyde and 1,1′-biphenyl-3-ylmethylamine hydrobromide gave the title compound as an oil. M+(LC/MS(ESI)): 496.5. HPLC (Condition A), Rt: 4.99 min (HPLC purity: 87.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592477B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-522650b048b24b079127066066627ee1 |
| Source note | uspto-grants-2009_09 |