Chlorotrimethylsilane → 2,2-Dimethyl-1-ethoxy-3-[(trimethylsilyl)oxy]propane

Reaction equation

[CH3:1][C:2]([CH3:9])([CH2:5][O:6][CH2:7][CH3:8])[CH2:3][OH:4].[CH3:10][Si:11](Cl)([CH3:13])[CH3:12]>>[CH3:1][C:2]([CH3:9])([CH2:3][O:4][Si:11]([CH3:13])([CH3:12])[CH3:10])[CH2:5][O:6][CH2:7][CH3:8]

Participants

Reactant 2

HCID 6397Chlorotrimethylsilane

HCID 126982853-Ethoxy-2,2-dimethylpropan-1-ol

Product 1

HCID 860800402,2-Dimethyl-1-ethoxy-3-[(trimethylsilyl)oxy]propane

Procedure

According to the procedure as described in Example 1,2,2-dimethyl-1-ethoxy-3-[(trimethylsilyl)oxy]propane was prepared from intermediate 2,2-dimethyl-3-ethoxy-1-propanol and reagent trimethylsilyl chloride.

Sources & evidence

ORD record: ord-7df1952d099640c0b7d4c5adedbefcfa
Source dataset: uspto-grants-2008_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07399812B2

Reaction notes

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