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4-(Methylthio)benzylamine → HCID 69155526, compound

HRID 750289
Notes
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Reaction equation

HRID 750289 reaction equation
[CH3:1][O:2][C:3]([C:5]1[O:6][C:7]([C:9]2[C:14]([C:15]=1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)=[CH:13][C:12]([Br:22])=[CH:11][CH:10]=2)=O)=[O:4].[CH3:23][S:24][C:25]1[CH:32]=[CH:31][C:28]([CH2:29][NH2:30])=[CH:27][CH:26]=1>>[CH3:1][O:2][C:3]([C:5]1[N:30]([CH2:29][C:28]2[CH:31]=[CH:32][C:25]([S:24][CH3:23])=[CH:26][CH:27]=2)[C:7](=[O:6])[C:9]2[C:14]([C:15]=1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)=[CH:13][C:12]([Br:22])=[CH:11][CH:10]=2)=[O:4]
ParticipantsProcedureWorkupSources & evidenceReaction notes

Participants

3

Reactant 2

HCID 27600804-(Methylthio)benzylamineHCID 66990710Methyl 6-bromo-1-oxo-4-phenyl-1H-isochromene-3-carboxylate

Product 1

HCID 69155526HCID 69155526, compound

Procedure

The present compound was synthesized by a method similar to that in Example 83 and using 6-bromo-4-phenyl-3-isocoumarincarboxylic acid methyl ester and 4-(methylthio)benzylamine.

Workup

  1. customThe present compound was synthesized by a method similar to that in Example 83

Sources & evidence

ORD record
ord-8dc19d9a03cd4987a48c1ae9d6b6411d
Source dataset
uspto-grants-2008_07
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US07402595B2

Reaction notes

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On this pageParticipantsProcedureWorkupSources & evidenceReaction notes