Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 7507Generated: October 23, 2026

Benzaldehyde → HCID 178419005, compound

https://huagongshe.com/en/reaction/7507

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantAcetyl chlorideHCID 6367—
Reactant2-AminopyridineHCID 10439—
ReactantTert-Butyl isocyanideHCID 23577—
SolventPerchloric AcidHCID 24247—
ProductHCID 178419005HCID 178419005—

Reaction Steps

Example 1 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07087607B2
Source datasetuspto-grants-2006_08
ORD IDord-cabf1b5deefc47dab71d1501ee332e9c
Source noteuspto-grants-2006_08