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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 7513Generated: October 23, 2026

Acetaldehyde → HCID 178418843, compound

https://huagongshe.com/en/reaction/7513

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetaldehydeHCID 177—
ReactantAcetyl chlorideHCID 6367—
ReactantCyclohexyl isocyanideHCID 79129—
Reactant2-Amino-3-benzyloxypyridineHCID 90334—
SolventPerchloric AcidHCID 24247—
ProductHCID 178418843HCID 178418843—

Reaction Steps

Example 7 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-3-benzyloxypyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07087607B2
Source datasetuspto-grants-2006_08
ORD IDord-efb2df06a3ae44799f8795ccf59d72ac
Source noteuspto-grants-2006_08