HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → HCID 178418843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Cyclohexyl isocyanide | HCID 79129 | — |
| Reactant | 2-Amino-3-benzyloxypyridine | HCID 90334 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 178418843 | HCID 178418843 | — |
Reaction Steps
Example 7 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-3-benzyloxypyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07087607B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-efb2df06a3ae44799f8795ccf59d72ac |
| Source note | uspto-grants-2006_08 |