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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 7517Generated: October 23, 2026

Benzaldehyde → HCID 178419071, compound

https://huagongshe.com/en/reaction/7517

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzaldehydeHCID 240—
ReactantOctanoyl chlorideHCID 8124—
Reactant2-AminopyridineHCID 10439—
ReactantTert-Butyl isocyanideHCID 23577—
SolventPerchloric AcidHCID 24247—
ProductHCID 178419071HCID 178419071—

Reaction Steps

Example 11 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process steps b) to d) by reacting the resultant reaction product with 0.4 mmol heptylcarboxylic acid chloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07087607B2
Source datasetuspto-grants-2006_08
ORD IDord-fed35cec3dc043e3b9de4b02712093a2
Source noteuspto-grants-2006_08