HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 178419071, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Octanoyl chloride | HCID 8124 | — |
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | Tert-Butyl isocyanide | HCID 23577 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | HCID 178419071 | HCID 178419071 | — |
Reaction Steps
Example 11 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyridine (0.1 M, DCM), 0.575 ml (0.115 mmol) tert.-butylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) benzaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process steps b) to d) by reacting the resultant reaction product with 0.4 mmol heptylcarboxylic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07087607B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-fed35cec3dc043e3b9de4b02712093a2 |
| Source note | uspto-grants-2006_08 |