HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4,5,6,7-tetrahydrobenzothiazole → 3-(2-methoxy-ethyl)-4,5,6,7-tetrahydro-3H-benzothiazol-2-ylideneamine hydrobromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4,5,6,7-tetrahydrobenzothiazole | HCID 18046 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Product | 3-(2-methoxy-ethyl)-4,5,6,7-tetrahydro-3H-benzothiazol-2-ylideneamine hydrobromide | HCID 66859028 | — |
Reaction Steps
A mixture of 4,5,6,7-tetrahydro-benzothiazol-2-ylamine (300 mg, 1.94 mmol) and 2-bromoethyl methyl ether (600 μL, 6.40 mmol) was processed according to the method of Example 12A to provide the title compound as crude product: MS (LC/MS) m/z 213 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08841334B2 |
| Source dataset | uspto-grants-2014_09 |
| ORD ID | ord-8847ec3281d5466a99cd84ae68050294 |
| Source note | uspto-grants-2014_09 |