HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 78488Generated: October 26, 2026
Allyl bromide → 3-allyl-4,5-dimethylthiazol-2(3H)-imine hydrobromide
https://huagongshe.com/reaction/78488
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| Solvent | Toluene | HCID 1140 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 3-allyl-4,5-dimethylthiazol-2(3H)-imine hydrobromide | HCID 68623542 | — |
Reaction Steps
A mixture of 4,5-dimethyl-1,3-thiazol-2-amine (1 g) and allylbromide (0.95 g) in toluene (5 mL) was heated to 85° C. for 12 hours, cooled, diluted with ether, filtered and the solvent was evaporated to afford crude product that was taken on to the next step without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08841334B2 |
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| Source dataset | uspto-grants-2014_09 |
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| ORD ID | ord-b550bf94e1dc44afbb8ef0c33f28bdba |
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| Source note | uspto-grants-2014_09 |
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