(6-Methoxypyridin-3-yl)boronic acid → 4-(6'-Methoxy-3,3'-bipyridin-5-yl)-1,4-diazatricyclo[4.3.1.13,8]undecane
Reaction equation
Br[C:2]1[CH:3]=[C:4]([N:8]2[CH2:16][CH:15]3[CH2:17][N:11]4[CH2:12][CH:13]([CH2:18][CH:9]2[CH2:10]4)[CH2:14]3)[CH:5]=[N:6][CH:7]=1.[CH3:19][O:20][C:21]1[CH:26]=[CH:25][C:24](B(O)O)=[CH:23][N:22]=1>>[CH3:19][O:20][C:21]1[N:22]=[CH:23][C:24]([C:2]2[CH:7]=[N:6][CH:5]=[C:4]([N:8]3[CH2:16][CH:15]4[CH2:17][N:11]5[CH2:12][CH:13]([CH2:18][CH:9]3[CH2:10]5)[CH2:14]4)[CH:3]=2)=[CH:25][CH:26]=1Participants
3
Procedure
The title compound was prepared from the product of Example 65A and 2-methoxypyridin-5-ylboronic acid according to General Method B: LC-MS Method D (ESI+) m/z 337.0 (M+H)+, retention time 1.23 minutes.
Sources & evidence
- ORD record
- ord-d1dadbd5521b40489220371ffe138f18
- Source dataset
- uspto-grants-2014_09