Ethyl bromoacetate → HCID 70847707, compound

Reaction equation

[F:1][C:2]1[CH:3]=[C:4]2[C:8](=[CH:9][CH:10]=1)[NH:7][N:6]=[CH:5]2.Br[CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14]>>[F:1][C:2]1[CH:10]=[CH:9][C:8]2[C:4](=[CH:5][N:6]([CH2:12][C:13]([O:15][CH2:16][CH3:17])=[O:14])[N:7]=2)[CH:3]=1

Participants

Reactant 2

HCID 7748Ethyl bromoacetate

HCID 178424865-Fluoro-1H-indazole

Product 1

HCID 70847707HCID 70847707, compound

Procedure

The title compound was prepared according to the method described for Preparation 93 using 5-fluoro-1H-indazole and ethyl bromoacetate to afford the title compound as an off-white solid in 27% yield, 130 mg.

Workup

customThe title compound was prepared

Sources & evidence

ORD record: ord-ff99cef28d064ddebb90f5cf78562b67
Source dataset: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08846698B2

Reaction notes

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