HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 4-Piperidinylbut-1-ene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Homoallyl bromide | HCID 21241 | — |
| Product | 4-Piperidinylbut-1-ene | HCID 4562282 | 93.4% |
Reaction Steps
4-Bromobut-1-ene (1.35 g) was treated with piperidine (1.7 g) and heated at reflux for 3 hours. The mixture was cooled to ambient temperature, filtered and the residue washed with ether (50 mL). The combined filtrate and washings were evaporated to give the title compound (1.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07087757B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-d7ef957ab1cf46f68f1f4c42cdc7ceea |
| Source note | uspto-grants-2006_08 |