Ethylenediamine → HCID 12635590, compound

Reaction equation

[CH2:1]([NH2:4])[CH2:2][NH2:3].[Br:5][C:6]1[CH:11]=[CH:10][CH:9]=[C:8]([Br:12])[C:7]=1[N:13]=[C:14]=[S:15]>>[NH2:3][CH2:2][CH2:1][NH:4][C:14]([NH:13][C:7]1[C:8]([Br:12])=[CH:9][CH:10]=[CH:11][C:6]=1[Br:5])=[S:15]

Participants

Reactant 2

HCID 3301Ethylenediamine

HCID 126355872,6-Dibromophenyl isothiocyanate

Product 1

HCID 12635590HCID 12635590, compound

Procedure

In a similar manner to that described in Example 1, ethylenediamine was reacted with 2,6-dibromophenylisothiocyanate to yield 1-(2-aminoethyl)-3-(2,6-dibromophenyl)thiourea, melting point 155°-157°.

Sources & evidence

ORD record: ord-e864364ba38c474193ca854d39d64621
Source dataset: uspto-grants-1978_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04096276

Reaction notes

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