5-(Ethylsulfonyl)-2-methoxybenzoic acid → HCID 20190709, compound

Reaction equation

[CH2:1]([S:3]([C:6]1[CH:7]=[C:8]([C:12]([O:15][CH3:16])=[CH:13][CH:14]=1)[C:9](O)=[O:10])(=[O:5])=[O:4])[CH3:2].ClC1C=C(Cl)C=CC=1C[NH:26]CCNCC>>[CH2:1]([S:3]([C:6]1[CH:7]=[C:8]([C:12]([O:15][CH3:16])=[CH:13][CH:14]=1)[C:9]([NH2:26])=[O:10])(=[O:5])=[O:4])[CH3:2]

Participants

Reactant 2

HCID 785565-(Ethylsulfonyl)-2-methoxybenzoic acid

HCID 20344799HCID 20344799, compound

Product 1

HCID 20190709HCID 20190709, compound

Procedure

By following general method B using 0.9 g. of 3-ethylsulfonyl-6-methoxybenzoic acid and 0.9 g. of N-(2',4'-dichlorophenylmethyl)-N'-ethylethylenediamine, 1.5 g. of N-[2-(N'-2',4'-dichlorophenylmethyl)-N'-ethylamino)ethyl]-3-ethylsulfonyl-6-methoxybenzamide was obtained.

Sources & evidence

ORD record: ord-1cf3acfcf41a427a8212a7edd515b906
Source dataset: uspto-grants-1978_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04097487

Reaction notes

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