Acetic Anhydride → 1-Chloro-4-acetoxy-8-methylnonane

Reaction equation

[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([OH:12])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:11])[CH3:10].[C:13](OC(=O)C)(=[O:15])[CH3:14]>>[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([O:12][C:13](=[O:15])[CH3:14])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:10])[CH3:11]

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 203222521-Chloro-8-methylnonan-4-OL

Product 1

HCID 203860491-Chloro-4-acetoxy-8-methylnonane

Procedure

A mixture of 1-chloro-8-methyl-4-nonanol (22.73 g.; 0.118 mole) and acetic anhydride (24.07 g.; 0.236 mole) is heated on a steam bath for 1-1/2 hours.

Workup

temperatureis heated on a steam bath for 1-1/2 hours

Sources & evidence

ORD record: ord-31223388004a436da058fa59794ee420
Source dataset: uspto-grants-1978_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04097504

Reaction notes

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