HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → (+)-4-(2-Methyldecanoyl) phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Decanoic acid, 2-methyl- | HCID 91167 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (+)-4-(2-Methyldecanoyl) phenol | HCID 53900693 | 40% |
Reaction Steps
Then, the same procedure as in Example 1 was repeated except that the above (+)-2-methyl decanoic acid was used instead of (+)-2-methyl butanoic acid to convert this compound into an acid chloride, which was reacted with phenol through aluminum chloride in methylene chloride to obtain (+)-4-(2-methyldecanoyl) phenol having the aforementioned physical and chemical properties at a yield of 40%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05137653 |
| Source dataset | uspto-grants-1992_08 |
| ORD ID | ord-7f0319ed762c4c32be7fbb428e598d7f |
| Source note | uspto-grants-1992_08 |