Ammonium Chloride → HCID 178479073, compound
Reaction equation
CO[C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH2:10][CH:11]=[CH:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[N:9]=1.[Cl-:19].[NH4+:20]>CO>[ClH:19].[C:13]1([CH:12]=[CH:11][CH2:10][CH:8]2[NH:9][C:3](=[NH:20])[CH2:4][CH2:5][CH2:6][CH2:7]2)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The product of Example 33 (0.50 g, 2.05 mmol) in 18 mL of MeOH was reacted with ammonium chloride (144 mg, 2.7 mmol) by the method of Example 5 to yield 258 mg (30%) of the title material.
Sources & evidence
- ORD record
- ord-1d3f31da0b7c4a7eb4d49cc9a3f6e4ea
- Source dataset
- uspto-grants-2000_01
- Patent number
- US06011028
Reaction notes
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