Sodium tetrachloroaurate → HCID 88265867, compound

HRID 849633

Reaction equation

HRID 849633 reaction equation
[Na+].Cl[Au-:3](Cl)(Cl)Cl.[SH:7][CH2:8][CH2:9][C:10]([NH:12][CH2:13][C:14]([OH:16])=[O:15])=[O:11]>O>[SH:7][CH2:8][CH2:9][C:10]([NH:12][CH2:13][C:14]([OH:16])=[O:15])=[O:11].[Au:3]

Participants

4

Reactant 2

HCID 27127Sodium tetrachloroaurateHCID 165505N-(1-Hydroxy-3-sulfanylpropylidene)glycine

Product 1

HCID 88265867HCID 88265867, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of sodium tetrachloroaurate (35g) in distilled water (200 ml) was slowly added to a solution of ethyl 2-hydroxethyl sulphide (20.5g) in distilled water (200 ml). Solid addition of mercaptopropionyl-glycine (5.21g) followed by vigorous stirring yielded gold mercaptopropionylglycine as a white solid (yield, based on gold, 85%).

Workup

  1. customyielded

Sources & evidence

ORD record
ord-e7d8fb6b736d4d7eaf139c73e883189b
Source dataset
uspto-grants-2000_01
Patent number
US06013798

Linked notes

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