HCID 12428590, compound → HCID 178443986, compound

Reaction equation

[CH2:1]([C:3]([N:8]=[C:9]=[N:10][C:11]1[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=1)([CH2:6][CH3:7])[CH2:4][CH3:5])[CH3:2].C([N:21]=[C:22]=[N:23]C1C=NC=CC=1)(C)(C)C>>[C:22]([N:23]=[C:9]([NH:10][C:11]1[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=1)[NH:8][C:3]([CH2:4][CH3:5])([CH2:6][CH3:7])[CH2:1][CH3:2])#[N:21]

Participants

Reactant 2

HCID 12428590HCID 12428590, compound

HCID 20501874HCID 20501874, compound

Product 1

HCID 178443986HCID 178443986, compound

Procedure

By following the procedure in Example 1, but substituting N-(1,1-diethylpropyl)-N'-3-pyridylcarbodiimide for the N-tert-butyl-N'-3-pyridylcarbodiimide, the N"-cyano-N-(1,1-diethylpropyl)-N'-3-pyridylguanidine was obtained with a melting point of 192.5°-193.5° C.

Sources & evidence

ORD record: ord-dc3019f8979343bf90ce8c9e967a50ac
Source dataset: uspto-grants-1983_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: USRE031244

Reaction notes

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