2-chloro-N,N-dimethylacetamide → N-allyl-S-(N,N-dimethylcarbamoylmethyl)thiouronium chloride

HRID 863724

Reaction equation

[CH2:1]([NH:4][C:5]([NH2:7])=[S:6])[CH:2]=[CH2:3].[Cl:8][CH2:9][C:10]([N:12]([CH3:14])[CH3:13])=[O:11]>>[Cl-:8].[CH2:1]([NH+:4]=[C:5]([NH2:7])[S:6][CH2:9][C:10](=[O:11])[N:12]([CH3:14])[CH3:13])[CH:2]=[CH2:3]

Participants

Reactant 2

HCID 758862-chloro-N,N-dimethylacetamide

HCID 1549517Allylthiourea

Product 1

HCID 19419964N-allyl-S-(N,N-dimethylcarbamoylmethyl)thiouronium chlorideYield 79%

Procedure

Example 1 was repeated with N-allylthiourea and 2-chloro-N,N-dimethylacetamide, affording the title compound in a yield of 79%.

Sources & evidence

ORD record: ord-f915d409404b4ff49efcc7a6125781b6
Source dataset: uspto-grants-1996_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05560814

Linked notes

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