HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → (4-Chloro-benzyl)-[3-(3-thieno[2,3-d]isoxazol-3-yl-phenoxy)-propyl]-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chlorobenzylamine | HCID 66036 | — |
| Reactant | 3-[3-(3-Chloro-propoxy)-phenyl]-thieno[2,3-d]isoxazole | HCID 21983556 | — |
| Reactant | 3-[3-(3-Bromo-propoxy)phenyl]-thieno[2,3-d]isoxazole | HCID 21983559 | — |
| Product | (4-Chloro-benzyl)-[3-(3-thieno[2,3-d]isoxazol-3-yl-phenoxy)-propyl]-amine | HCID 21983591 | — |
Reaction Steps
The title compound is prepared from a mixture of 3-[3-(3-bromo-propoxy)phenyl]-thieno[2,3-d]isoxazole, 3-[3-(3-chloro-propoxy)-phenyl]-thieno[2,3-d]isoxazole, 4-chlorobenzylamine and potassium carbonate essentially as described above in example 4. Purity by LC/MS (APCI)=100%, [M+H]+=399 m/e.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091199B1 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-753b8f4b0e8840059f919aa58a8e8fe8 |
| Source note | uspto-grants-2006_08 |