Ethanolamine → Ethanolamine trans-traumatate

HRID 865831

Reaction equation

HRID 865831 reaction equation
[C:1]([OH:16])(=[O:15])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13].[CH2:17]([CH2:19][NH2:20])[OH:18]>O>[C:1]([OH:16])(=[O:15])/[CH:2]=[CH:3]/[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][C:12]([OH:14])=[O:13].[CH2:17]([CH2:19][NH2:20])[OH:18]

Participants

4

Reactant 2

HCID 700EthanolamineHCID 5283028Traumatic Acid

Product 1

HCID 131719631Ethanolamine trans-traumatate

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

2.28 g of trans-traumatic acid (10 mmol) are suspended in 100 ml of water at 4° C. A solution of 1.23 g ethanolamine as free base in 20 ml water, under continuous stirring is slowly added drop by drop in 30 minutes to the resulting suspension.

Workup

  1. customin 30 minutes

Sources & evidence

ORD record
ord-9823ff988bf9452a90c3750d2d05b2b2
Source dataset
uspto-grants-1996_10
Patent number
US05567716

Linked notes

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