AGN-PC-0NC49B → HCID 14273353, compound
Reaction equation
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:16])([CH3:15])[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:16])([CH3:15])[CH2:8][C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
112.5 g of trimethylbenzylammonium monomethylcarbonate and 55.0 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylbenzylammonium hydrogencarbonate was obtained in a yield of 95.7 mol %.
Workup
- customas used in Preparation Example 1
- temperatureheated
- customreached 120° C.
Sources & evidence
- ORD record
- ord-7f7da973e61b4a93aa39d8f9bc886d11
- Source dataset
- uspto-grants-1988_10
- Patent number
- US04776929
Reaction notes
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