HCID 19871551, compound → HCID 85570074, compound
Reaction equation
C[O:2][C:3](=[O:5])[O-:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]>O>[C:3](=[O:2])([O-:5])[OH:4].[CH3:6][N+:7]([CH3:11])([CH3:10])[CH2:8][CH3:9]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
114.1 g of trimethylethylammonium monomethylcarbonate and 75.6 g of water were introduced in the same reactor as used in Preparation Example 1 and heated with stirring. After the temperature in the reactor reached 120° C., the reaction was continued for 3 hours at 120° C. Trimethylethylammonium hydrogencarbonate was obtained in a yield of 96.3 mol %.
Workup
- customas used in Preparation Example 1
- temperatureheated
- customreached 120° C.
Sources & evidence
- ORD record
- ord-13ae56ff8ff94768903a653a32d808d9
- Source dataset
- uspto-grants-1988_10
- Patent number
- US04776929
Reaction notes
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