HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,7-Diphenyl-4-heptanol → HCID 178418375, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,7-Diphenyl-4-heptanol | HCID 10539870 | — |
| Reactant | HCID 178418459 | HCID 178418459 | — |
| Reactant | HCID 178418471 | HCID 178418471 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178418375 | HCID 178418375 | — |
Reaction Steps
The alcohol 137 was prepared from the crude aldehyde 136. and 1.5 mL (0.75 mmol) of 120 in 2.0 mL of THF as described above for the synthesis of alcohol 121 in Example 1 to give 220 mg of the crude diastereomeric alcohol 137. Flash chromatography (elution with 20% ethyl acetate in hexane) afforded 146 mg of the alcohol 137 as an oil. 1H NMR consistent with structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723459 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-a6be5895ebf2488a874923e3878acfbe |
| Source note | uspto-grants-1998_03 |