Dimethyl Sulfate → 2-Bromo-7-methoxynaphthalene

HRID 891958

Reaction equation

[Br:1][C:2]1[CH:11]=[C:10]2[C:5]([CH:6]=[CH:7][C:8]([OH:12])=[CH:9]2)=[CH:4][CH:3]=1.[CH3:13]OS(OC)(=O)=O>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]2[C:10](=[CH:9][C:8]([O:12][CH3:13])=[CH:7][CH:6]=2)[CH:11]=1

Participants

Reactant 2

HCID 6497Dimethyl Sulfate

HCID 6138277-Bromo-2-naphthol

Product 1

HCID 129927592-Bromo-7-methoxynaphthalene

Procedure

The title compound, MS: m/e=236(M+), was prepared from 7-bromo-naphth-2-ol and dimethylsulfate following the procedure described in example 162.

Sources & evidence

ORD record: ord-e553e72bd96147389afad4caeb5dc73f
Source dataset: uspto-grants-2006_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07005432B2

Linked notes

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