HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-(4-chlorophenyl)furan-2-carbonyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-(4-Chlorophenyl)-2-furoic acid | HCID 726693 | — |
| Product | 5-(4-chlorophenyl)furan-2-carbonyl Chloride | HCID 2771970 | — |
Reaction Steps
A mixture of 56 g. (0.25 mole) of 5-(p-chlorophenyl)-2-furoic acid and 100 ml. of SOCl2 is refluxed for 31/2 hours so that HCl gas evolves and there is dissolution. The SOCl2 is removed on a rotary evaporator. Benzene is added to the solid residue and is then removed on the rotary evaporator to give 5-(p-chlorophenyl)-2-furoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118708 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-0765c2512ca14c33837126d1b45c10ff |
| Source note | uspto-grants-1992_06 |