Chloro(phenyl)acetyl chloride → HCID 15691788, compound

HRID 893338

Reaction equation

[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([NH2:8])=[S:7])=[CH:4][CH:3]=1.Cl[CH:12]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)[C:13](Cl)=[O:14]>>[CH3:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]2[S:7][C:12]([C:16]3[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=3)=[C:13]([OH:14])[N:8]=2)=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 102902Chloro(phenyl)acetyl chloride

HCID 7372094-Methylbenzenecarbothioamide

Product 1

HCID 15691788HCID 15691788, compound

Procedure

The title compound was prepared according to the method of Scheme II in a manner analogous to Example 31 except 4-methylthiobenzamide was used instead of thiobenzamide and 2-chloro-2-phenylacetyl chloride was used instead of 2-bromopropionate.

Sources & evidence

ORD record: ord-718fd806b40a463197f9376d32bf09f1
Source dataset: uspto-grants-1992_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05124342

Linked notes

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