5-chlorobenzothiophene → HCID 86745959, compound

HRID 893853

Reaction equation

HRID 893853 reaction equation
[CH2:1]([O:3][C:4]([CH:6]1[CH:14]2[C:9]3([CH:18]=[CH:17][CH:16]=[CH:15][C:10]3=[N:11][CH2:12][CH2:13]2)[S:8][CH2:7]1)=[O:5])[CH3:2].[Cl:19]C1C=CC2SC=CC=2C=1>>[CH2:1]([O:3][C:4]([CH:6]1[CH:14]2[C:9]3([CH:18]=[CH:17][CH:16]=[CH:15][CH:10]3[N:11]([Cl:19])[CH2:12][CH2:13]2)[S:8][CH2:7]1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 113097545-chlorobenzothiopheneHCID 199609281,2,3,4-Tetrahydro-benzo[b]thieno[2,3,c]pyridine-3-carboxylic acid ethyl ester

Product 1

HCID 86745959HCID 86745959, compound

Procedure

6-Chloro-1,2,3,4-tetrahydro-benzo[b]thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester was synthesized by following the same procedure as the synthesis of 1,2,3,4-tetrahydro-benzo[b]thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester in Example 1 except that 42.3 g of 5-chlorobenzothiophene was used in place of 33.6 g of benzothiophene in Example 1.

Sources & evidence

ORD record
ord-5f19cf0bf0c8423883f6990c3e1d1f31
Source dataset
uspto-grants-1992_06
Patent number
US05126448

Linked notes

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