Reaction equation
O[CH2:2][NH:3][C:4](=[O:8])[C:5]([CH3:7])=[CH2:6].[C:9]1([P:15]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)([SH:17])=[S:16])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[C:9]1([P:15]([C:18]2[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=2)([S:17][CH2:2][NH:3][C:4](=[O:8])[CH:5]([CH3:7])[CH2:6][S:17][P:15]([C:18]2[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=2)([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=2)=[S:16])=[S:16])[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1Participants
3
Procedure
Following the general procedure in Example 1, 0.4 mole N-hydroxymethylmethacrylamide is reacted with 0.08 mole of diphenylphosphinodithioic acid, to yield N-(diphenylphosphinothioylthiomethyl) 3-(diphenylphosphinothioylthio)-2-methylpropionamide.
Sources & evidence
- ORD record
- ord-c62fe282e14c4dbfaa57c501435b6359
- Source dataset
- uspto-grants-1981_08
- Patent number
- US04282171
Linked notes
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