Methanol → HCID 59896206, compound

Reaction equation

[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([OH:10])=[O:9])[NH2:7].[CH3:11]O>>[NH2:1][CH2:2][CH2:3][S:4][CH2:5][C@@H:6]([C:8]([O:10][CH3:11])=[O:9])[NH2:7]

Participants

Reactant 2

HCID 887Methanol

HCID 99558S-(2-Aminoethyl)-L-cysteine

Product 1

HCID 59896206HCID 59896206, compound

Procedure

A 10 g (50 mmol) sample of S-(2-aminoethyl)-L-cysteine was dissolved in 400 mL of methanol. Into this cooled solution was bubbled in anhydrous HCl for 30 minutes. After stirring at room temperature overnight, the solution was concentrated to afford 12.7 g of the title compound.

Workup

customInto this cooled solution was bubbled in anhydrous HCl for 30 minutes
concentrationthe solution was concentrated

Sources & evidence

ORD record: ord-0086953fef694a4197e1077e07363b4c
Source dataset: uspto-grants-2005_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06914158B2

Reaction notes

Loading…