HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 1-(2-Methyl-benzylidene)-piperidinium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 2-Methylbenzaldehyde | HCID 10722 | — |
| Product | 1-(2-Methyl-benzylidene)-piperidinium chloride | HCID 17912257 | — |
Reaction Steps
The reaction of 9.5 ml (0.096 mol) piperidine and 4.7 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 2 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.8 g (corresponding to 65% of the yield calculated by theory) 1-(2-methyl-benzylidene)-piperidinium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091220B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-00adf1ba992d4cb99f816842b438f344 |
| Source note | uspto-grants-2006_08 |