HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → (2-Methyl-benzylidene)-dimethylammonium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-Methylbenzaldehyde | HCID 10722 | — |
| Product | (2-Methyl-benzylidene)-dimethylammonium chloride | HCID 21985341 | — |
Reaction Steps
The reaction of 14.0 ml (0.108 mol) dimethylamine solution and 4.6 ml (0.040 mol) 2-methylbenzaldehyde in accordance with general synthesis instructions 1 and subsequent reaction with 2.4 ml (0.040 mol) acetyl chloride in accordance with general synthesis instructions 3 gave 5.3 g (corresponding to 73% of the yield calculated by theory) dimethyl-(2-methyl-benzylidene)-ammonium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07091220B2 |
| Source dataset | uspto-grants-2006_08 |
| ORD ID | ord-9d6a01b849784a7f99927f8025b4abe7 |
| Source note | uspto-grants-2006_08 |