Carbon Dioxide → HCID 178514403, compound

HRID 905513

Reaction equation

HRID 905513 reaction equation
[N:1]([CH2:10][C:11]([OH:13])=[O:12])([CH2:6][C:7]([OH:9])=[O:8])[CH2:2][C:3]([OH:5])=[O:4].C(=O)(O)O.[NH2:18][NH:19][C:20]([NH2:22])=[NH:21].C(=O)=O>O>[N:1]([CH2:2][C:3]([O-:5])=[O:4])([CH2:6][C:7]([O-:9])=[O:8])[CH2:10][C:11]([O-:13])=[O:12].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21].[NH2:18][NH:19][C:20]([NH2:22])=[NH2+:21]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 8758Nitrilotriacetic AcidHCID 178513185HCID 178513185, compound

Product 1

HCID 178514403HCID 178514403, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Nitrilotriacetic acid (1.0 g, 5.23 mmol) was dissolved in 10 ml of distilled water. Aminoguanidine bicarbonate (2.14 g, 15.69 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for three days. The water was removed in vacuo with heating to approximately 90° C. The product was isolated as a white solid.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C
  3. customThe product was isolated as a white solid

Sources & evidence

ORD record
ord-3a1b04a135ae49119311cf305d8c8721
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Linked notes

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