Acetylacetone → tetrakis((Z)-4-hydroxypent-3-en-2-one);titanium

HRID 905526

Reaction equation

HRID 905526 reaction equation

[C:1]([CH2:4][C:5](=[O:7])[CH3:6])(=[O:3])[CH3:2].CCO.CCO.CCO.CCO.[Ti:20]>>[CH3:6]/[C:5](/[OH:7])=[CH:4]/[C:1]([CH3:2])=[O:3].[CH3:6]/[C:5](/[OH:7])=[CH:4]/[C:1]([CH3:2])=[O:3].[CH3:6]/[C:5](/[OH:7])=[CH:4]/[C:1]([CH3:2])=[O:3].[CH3:6]/[C:5](/[OH:7])=[CH:4]/[C:1]([CH3:2])=[O:3].[Ti:20]

Participants

3

Reactant 2

HCID 31261Acetylacetone

HCID 2724286Titanium(IV)ethoxide

Product 1

HCID 44629996tetrakis((Z)-4-hydroxypent-3-en-2-one);titanium

Procedure

1 g of acetylacetone and 1 g of tetraethyl orthotitanate were added to the hydrophilic sol-gel liquid to prepare it,

Workup

customto prepare it

Sources & evidence

ORD record: ord-05773a22f5d243d49954dfd4b1db41bf
Source dataset: uspto-grants-2011_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08012591B2

Linked notes

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