Hydrazine → HCID 27055575, compound
Reaction equation
[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([O:14]CC)=O.[NH2:17][NH2:18]>C(O)C>[CH2:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH2:4][CH2:3][N:2]1[CH2:11][C:12]([NH:17][NH2:18])=[O:14]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 90 (2.0 g, 9.12 mmol) and hydrazine (5.1 g, 91 mmol) in ethanol (30 mL) was heated at reflux overnight. The mixture was concentrated under reduced pressure to give 91 (1.87 g ˜100%) which was used without further purification.
Workup
- temperatureat reflux overnight
- concentrationThe mixture was concentrated under reduced pressure
Sources & evidence
- ORD record
- ord-62c165ed74a74b769d7b88b2dc611239
- Source dataset
- uspto-grants-2007_09
- Patent number
- US07265122B2
Reaction notes
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