3-Chloropropanesulphonyl chloride → 5-(3-Chloropropylsulfonyl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

HRID 961

Reaction equation

HRID 961 reaction equation
[O:1]1[C:7]2[CH:8]=[CH:9][CH:10]=[CH:11][C:6]=2[NH:5][CH2:4][CH2:3][CH2:2]1.[Cl:12][CH2:13][CH2:14][CH2:15][S:16](Cl)(=[O:18])=[O:17]>>[Cl:12][CH2:13][CH2:14][CH2:15][S:16]([N:5]1[C:6]2[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=2[O:1][CH2:2][CH2:3][CH2:4]1)(=[O:18])=[O:17]

Participants

3

Reactant 2

HCID 154103-Chloropropanesulphonyl chlorideHCID 5777522,3,4,5-Tetrahydro-1,5-benzoxazepine

Product 1

HCID 196942775-(3-Chloropropylsulfonyl)-2,3,4,5-tetrahydro-1,5-benzoxazepine

Procedure

2,3,4,5-tetrahydro-1,5-benzoxazepine and 3-chloropropanesulfonyl chloride were used to produce the above compound in the same way as Reference Example 8.

Workup

  1. customto produce the above compound in the same way as Reference Example 8

Sources & evidence

ORD record
ord-962a1ba5fe544c1c818dea60c177a4b0
Source dataset
uspto-grants-1998_03
Patent number
US05723475

Linked notes

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