Acrolein → 4-Methyl-2-vinyl-1,3-dioxane

HRID 971598

Reaction equation

HRID 971598 reaction equation
[CH:1]([CH:3]=[CH2:4])=[O:2].[CH2:5](O)[CH2:6][CH:7]([OH:9])[CH3:8]>>[CH:3]([CH:1]1[O:9][CH:7]([CH3:8])[CH2:6][CH2:5][O:2]1)=[CH2:4]

Participants

3

Reactant 2

HCID 7847AcroleinHCID 78961,3-Butanediol

Product 1

HCID 1108964-Methyl-2-vinyl-1,3-dioxane

Procedure

Acrolein and 1,3-butanediol were condensed to produce 2-vinyl-4-methyl-1,3-dioxane in accordance with the procedure of Example I.

Workup

  1. customcondensed

Sources & evidence

ORD record
ord-c11899d7b11448bfb40275bc521652bd
Source dataset
uspto-grants-1979_07
Patent number
US04160771

Linked notes

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