Acetamidine → N'-[(2,6-dichlorostyryl)sulfonyl]acetamidine

HRID 972299

Reaction equation

[C:1]([NH2:4])(=[NH:3])[CH3:2].[Cl:5][C:6]1[CH:17]=[CH:16][CH:15]=[C:14]([Cl:18])[C:7]=1[CH:8]=[CH:9][S:10](Cl)(=[O:12])=[O:11]>>[Cl:5][C:6]1[CH:17]=[CH:16][CH:15]=[C:14]([Cl:18])[C:7]=1[CH:8]=[CH:9][S:10]([N:3]=[C:1]([NH2:4])[CH3:2])(=[O:12])=[O:11]

Participants

Reactant 2

HCID 67171Acetamidine

HCID 541116992,6-Dichlorostyrylsulfonyl chloride

Product 1

HCID 54372284N'-[(2,6-dichlorostyryl)sulfonyl]acetamidine

Procedure

Reaction of acetamidine with 2,6-dichlorostyrylsulfonyl chloride according to the procedure of Example 29 (b) affords N'-[(2,6-dichlorostyryl)sulfonyl]acetamidine, m.p. 154.5°-158.5° C. (corr.), from absolute ethanol.

Sources & evidence

ORD record: ord-c048d0a4ec6d4d3f9fac6060feeec184
Source dataset: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04052455

Linked notes

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