HCID 20263934, compound → HCID 20263985, compound
Reaction equation
[CH3:1][C:2]1[CH:7]=[C:6]([CH2:8][O:9][C:10](=[O:12])[CH3:11])[C:5]([CH2:13][OH:14])=[CH:4][N:3]=1>N1C=CC=CC=1.[O-2].[O-2].[O-2].[Cr+6]>[CH3:1][C:2]1[CH:7]=[C:6]([CH2:8][O:9][C:10](=[O:12])[CH3:11])[C:5]([CH:13]=[O:14])=[CH:4][N:3]=1Participants
4
Reactant 1
Product 1
Reagents, catalysts & solvents 2
Procedure
This product is prepared by oxidation of 2-methyl-4-acetoxymethyl-5-hydroxymethylpyridine (from Step A) with chromium trioxide in pyridine by the procedure substantially as described in Example 6, Step A.
Sources & evidence
- ORD record
- ord-d3e4ddce07134dbd8fa37a8863de4641
- Source dataset
- uspto-grants-1977_10
- Patent number
- US04053606
Reaction notes
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