2-Butanamine, 2-methyl- → Tertiaryamylaminoethoxyethanol

Reaction equation

[C:1]([NH2:6])([CH2:4][CH3:5])([CH3:3])[CH3:2].Cl[CH2:8][CH2:9][O:10][CH:11]([OH:13])[CH3:12]>>[C:1]([NH:6][CH2:8][CH2:9][O:10][CH:11]([OH:13])[CH3:12])([CH2:4][CH3:5])([CH3:3])[CH3:2]

Participants

Reactant 2

HCID 689862-Butanamine, 2-methyl-

HCID 221454452-Chloroethoxyethanol

Product 1

HCID 118893105TertiaryamylaminoethoxyethanolYield 66.7%

Procedure

In the manner described in Example 8, 129.7 g of tertiaryamylamine and 92.2 g of 2-chloroethoxyethanol yielded 86.5 g of tertiaryamylaminoethoxyethanol having a b.p. of 124° C. (10 mm).

Sources & evidence

ORD record: ord-b08368670a944f609ed53ddd47962eaa
Source dataset: uspto-grants-1987_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04665234

Reaction notes

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