Sec-Butylamine → Secondarybutylaminoethoxyethanol

Reaction equation

[CH:1]([NH2:5])([CH2:3][CH3:4])[CH3:2].Cl[CH2:7][CH2:8][O:9][CH:10]([OH:12])[CH3:11]>>[CH:1]([NH:5][CH2:7][CH2:8][O:9][CH:10]([OH:12])[CH3:11])([CH2:3][CH3:4])[CH3:2]

Participants

Reactant 2

HCID 24874Sec-Butylamine

HCID 221454452-Chloroethoxyethanol

Product 1

HCID 131713683SecondarybutylaminoethoxyethanolYield 60.6%

Procedure

In the manner described in Example 8, 131 g of secondarybutylamine and 93 g of 2-chloroethoxyethanol yielded 73 g of secondarybutylaminoethoxyethanol having a b.p. 120° C. (10 mm). Analysis calculated for C8H19NO2 : %N, 8.70: Found: %N, 8.45.

Sources & evidence

ORD record: ord-0bd13d9965ca4d35809b6e9b09d0ef79
Source dataset: uspto-grants-1987_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04665234

Reaction notes

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