HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethoxysilane → 1,14-Bis(triethoxysilyl)tetradecane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethoxysilane | HCID 13830 | — |
| Reactant | Tetradeca-1,13-diene | HCID 30875 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | 1,14-Bis(triethoxysilyl)tetradecane | HCID 22559811 | — |
Reaction Steps
A mixture of 25 g of 1,13-tetradecadiene (Aldrich), 44.4 g of triethoxysilane (Shin-Etsu Silicone) and 0.1 mL of 3% xylene solution of a platinum complex of bis((vinyl dimethyl)disiloxane) was stirred at room temperature in a nitrogen atmosphere for 3 days. The resultant reaction mixture was purified by distillation, to obtain 1,14-bis(triethoxysilyl)tetradecane. Its structure was confirmed by NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06864006B2 |
| Source dataset | uspto-grants-2005_03 |
| ORD ID | ord-6b9d9ed70234478894a9c99f754256de |
| Source note | uspto-grants-2005_03 |