HCID 86589079, compound → HCID 51360252, compound
Reaction equation
[N:1]([CH2:4][C@H:5]1[O:9][C@@H:8]([N:10]2[CH:25]=[CH:24][C:14]([NH:15]C(=O)C3C=CC=CC=3)=[N:13][C:11]2=[O:12])[C@H:7]([OH:26])[C@@H:6]1[OH:27])=[N+]=[N-]>N>[NH2:1][CH2:4][C@H:5]1[O:9][C@@H:8]([N:10]2[CH:25]=[CH:24][C:14]([NH2:15])=[N:13][C:11]2=[O:12])[C@H:7]([OH:26])[C@@H:6]1[OH:27]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
Then, the thus-obtained 5′-amino-5′-deoxy-N4-benzoylcytidine (8.5 g, 24.5 mmol) was dissolved in 28% aqueous ammonia (200 ml), and the mixture was stirred at room temperature for 24 hours. The solution was evaporated to dryness, and acetone was added to recover 5′-amino-5′-deoxycytidine (5.76 g, yield 97%).
Workup
- customThe solution was evaporated to dryness, and acetone
- additionwas added
Sources & evidence
- ORD record
- ord-50356b842ae44e948c3349d5689b5f92
- Source dataset
- uspto-grants-2005_03
- Patent number
- US06872809B2
Reaction notes
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