HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-1-butanol → N-(phenylacetyl)valine 2-methylbutyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-1-butanol | HCID 8723 | — |
| Reactant | (2S)-3-methyl-2-(2-phenylacetamido)butanoic acid | HCID 853958 | — |
| Product | N-(phenylacetyl)valine 2-methylbutyl Ester | HCID 15481773 | — |
Reaction Steps
Following General Procedure BC and using the N-(phenylacetyl)valine prepared in Step A above and 2-methylbutan-1-ol (Aldrich), the title compound was prepared as a diastereomeric mixture. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06632811B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-dd4e96332c8d4cb1a1d13b9d3530f049 |
| Source note | uspto-grants-2003_10 |