HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-chloropyridine → N-(5-Chloropyridin-2-yl)-4-methoxycarbonyl-2-nitrobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-chloropyridine | HCID 66174 | — |
| Reactant | 4-(Methoxycarbonyl)-2-nitrobenzoic acid | HCID 21906474 | — |
| Product | N-(5-Chloropyridin-2-yl)-4-methoxycarbonyl-2-nitrobenzamide | HCID 21906271 | 74% |
Reaction Steps
Using a similar procedure to that described in Example 1-A, 4-methoxycarbonyl-2-nitrobenzoic acid (1.87 g, 8.31 mmol) and 2-amino-5-chloropyridine (1.16 g, 9.14 mmol) afforded 2.05 g (74%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06635657B1 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-2f82940ef3da416d9419900ed14144db |
| Source note | uspto-grants-2003_10 |