HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-Butyl isocyanide → (2-Anthracen-9-yl-imidazo[1,2-a]pyrazin-3-yl)-tert-butyl-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-Butyl isocyanide | HCID 23577 | — |
| Reactant | 9-Anthracenecarboxaldehyde | HCID 69504 | — |
| Reactant | Aminopyrazine | HCID 78747 | — |
| Solvent | Perchloric Acid | HCID 24247 | — |
| Product | (2-Anthracen-9-yl-imidazo[1,2-a]pyrazin-3-yl)-tert-butyl-amine | HCID 17937207 | — |
Reaction Steps
Compound (30) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyrazine solution (0.1 M, MC), 0.575 ml tert-butyl isocyanide solution (0.2 M, MC), 0.500 ml anthracene-9-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 366.5; found mass 367.3 (ESI-MS)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06638933B2 |
| Source dataset | uspto-grants-2003_10 |
| ORD ID | ord-37a8b151357044feb540d0a6fe07f897 |
| Source note | uspto-grants-2003_10 |