3-[(5-Methyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester → 3-[(5-Methyl-furan-2-ylmethyl)-amino]-phthalic acid

HRID 10032

反応式

HRID 10032 の反応式
C[O:2][C:3](=[O:22])[C:4]1[C:5](=[C:10]([NH:14][CH2:15][C:16]2[O:17][C:18]([CH3:21])=[CH:19][CH:20]=2)[CH:11]=[CH:12][CH:13]=1)[C:6]([O:8]C)=[O:7].COCCNC1C=CC=C(C(O)=O)C=1C(O)=O>>[CH3:21][C:18]1[O:17][C:16]([CH2:15][NH:14][C:10]2[CH:11]=[CH:12][CH:13]=[C:4]([C:3]([OH:22])=[O:2])[C:5]=2[C:6]([OH:8])=[O:7])=[CH:20][CH:19]=1

参加物

3

反応物 2

HCID 210401293-[(5-Methyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl esterHCID 219885193-(2-Methoxy-ethylamino)-phthalic acid

生成物 1

HCID 219885393-[(5-Methyl-furan-2-ylmethyl)-amino]-phthalic acid

実験手順

3-[(5-Methyl-furan-2-ylmethyl)-amino]-phthalic acid dimethyl ester (5 mmol) was treated in the same manner as described above for the synthesis of 3-(2-methoxy-ethylamino)-phthalic acid. The product of the reaction, which contained a mixture of diacid and monomethyl esters, was used without further purification.

後処理

  1. customThe product of the reaction, which
  2. customwas used without further purification

出典と根拠

ORDレコード
ord-f38173b9cff244909a2e1e470e0343b6
出典データセット
uspto-grants-2006_08
特許番号
US07091353B2

関連ノート

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