化工社化工社 化学情報印刷レポート · 研究参考用
2-Methoxybenzaldehyde → alpha-(2-methoxyphenyl)-N-t-butylnitrone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methoxybenzaldehyde | HCID 8658 | — |
| 反応物 | N-tert-butylhydroxylamine | HCID 98586 | — |
| 生成物 | alpha-(2-methoxyphenyl)-N-t-butylnitrone | HCID 85447185 | — |
反応手順
The title compound was prepared according to the procedure described in Example 7 using 2-methoxybenzaldehyde and N-tert-butylhydroxylamine. The title compound was isolated in 82.9% overall yield as white crystals, m.p. 109.1 ° C. (Rf =0.53 on a silica gel plate using ethyl acetate as the eluant).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06046232 |
| 出典データセット | uspto-grants-2000_04 |
| ORD ID | ord-619ea8b4edd344849d580107504db57f |
| 出典メモ | uspto-grants-2000_04 |